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1 article(s) from Anjaneyulu, G S R

Identification and synthesis of impurities formed during sertindole preparation

I. V. Sunil Kumar,
G. S. R. Anjaneyulu and
V. Hima Bindu

Beilstein J. Org. Chem. 2011, 7, 29–33, doi:10.3762/bjoc.7.5

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Graphical Abstract

Figure 1: Sertindole (1), process related impurities and metabolites.

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Scheme 1: Reagents and conditions: i) K₂CO₃, CuBr, ethylenediamine, DMF 130–135 °C; ii) CH₃COOH, CF₃COOH, 100...

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Scheme 2: Reagents, conditions (and yields): i) (a) pH adjusted to 6; (b) Pd/C, HCOONH₄, AcOH, MeOH, reflux (...

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Scheme 3: Reagents, conditions (and yields): i) 16, K₂CO₃, KI, MIBK, reflux (73.9%).

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Scheme 4: Reagents, conditions (and yields): i) Cs₂CO₃, DMF, 130–135 °C; ii) 14, CH₃COOH, CF₃COOH, 100–105 °C...

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Scheme 5: Reagents, conditions (and yields): i) (a) pH adjusted to 6–7; (b) H₂, PtO₂, MeOH, AcOH, 30–35 °C (7...

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Scheme 6: Reagents, conditions (and yields): i) 12, K₂CO₃, Cu(II)Br, ethylenediamine, DMF, 130–135 °C, (51%);...

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Scheme 7: Reagents, conditions (and yield): i) (a) 16, Et₃N, NaI, CH₃CN, reflux; (b) column chromatography (1...

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Scheme 8: Reagents, conditions (and yield): i) (a) mCPBA, MeOH, 40–45 °C; (b) column chromatography (52.2%).

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Published 07 Jan 2011

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